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Beilstein J. Org. Chem. 2024, 20, 162–169, doi:10.3762/bjoc.20.15
Graphical Abstract
Scheme 1: The Hock rearrangement: (a) General mechanism (substituents are omitted); (b) Example of previous t...
Scheme 2: One-pot conversion of substrate 1 into dihydronaphthalene 4.
Scheme 3: One-pot conversion of substrate 1 into 1-aryltetraline structure 6, and the proposed mechanism for ...
Figure 1: X-ray crystallographic structure of product 6 (CCDC 2301977). The structure shows one disordered et...
Scheme 4: Free-energy profile of the hypothesized [1,5]-sigmatropic hydrogen shift between 7 and 7’, (IEFPCM(...
Figure 2: Examples of cyclolignan natural products [25-27].
Scheme 5: Scope of substrates and aromatic nucleophiles in the one-pot transformation. aNot determined (mixtu...
Beilstein J. Org. Chem. 2023, 19, 428–433, doi:10.3762/bjoc.19.32
Figure 1: Structure of latrunculins (the red dots show the natural product stereopentade).
Figure 2: General strategy for latrunculin cycle disconnections (left), previous works towards linear precurs...
Scheme 1: Synthesis of fragment 15 from (+)-β-citronellene (10).
Scheme 2: Synthesis of fragment 8 from ʟ-cysteine ethyl ester hydrochloride (16).
Scheme 3: Synthesis of fragment 21 through a stereoselective aldol reaction.
Scheme 4: 1,3-Anti-diastereoselective reduction of 21 with PNBz transposition, and final determination of the...